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Sol-gel synthesis and characterization of TiO2 powder

Year 2017, Volume: 1 Issue: 2, 38 - 40, 12.12.2017

Omer Kaygili Niyazi Bulut Cengiz Tatar Tankut Ates Turan İnce

Abstract

In the present study, TiO2
powder having the tetragonal crystal without any impurity was easily
synthesized by sol-gel method, and its characterization was done by X-ray
diffraction (XRD), scanning electron microscopy (SEM) and energy dispersive
X-ray (EDX) spectroscopy. The crystallinity degree was found to be of 89.0%. A
flaky morphology was observed.

Keywords

Sol-gel synthesis TiO2 X-ray diffraction (XRD)

References

  • Chimupala Y, Hyett G, Simpson R, Mitchell R, Douthwaite R, Milne SJ, Brydson RD. Synthesis and characterization of mixed phase anatase TiO2 and sodium-doped TiO2(B) thin films by low pressure chemical vapour deposition (LPCVD). RSC Adv 2014;4:48507-15.
  • Viana MM, Soares VF, Mohallem NDS. Synthesis and characterization of TiO2 nanoparticles. Ceram Int 2010;36:2047-53.
  • Dadkhah M, Salavati-Niasari M, Mir N. Synthesis and characterization of TiO2 nanoparticles by using new shape controllers and its application in dye sensitized solar cells. J Ind Eng Chem 2014;20:4039-44.
  • Paunović P, Grozdanov A, Češnovar A, Makreski P, Gentile G, Ranguelov B, Fidančevska E. Characterization of nanoscaled TiO2 produced by simplified sol–gel method using organometallic precursor. J Eng Mater Technol 2015;137:021003 1-5.
  • Byranvand MM, Kharat AN, Fatholahi L, Beiranvand ZM. A review on synthesis of nano-TiO2 via different methods. J Nanostruct 2013;3:1-9.
  • Li Z, Kawashita M, Doi M. Sol–gel synthesis and characterization of magnetic TiO2 microspheres. J Ceram Soc Jpn 2010;118:467-73.
  • Chen X, Mao SS. Titanium dioxide nanomaterials: Synthesis, properties, modifications, and applications. Chem Rev 2007;107:2891-959.
  • Phonkhokkong T, Thongtem T, Thongtem S, Phuruangrat A, Promnopas W. Synthesis and characterization of TiO2 nanopowders for fabrication of dye sensitized solar cells. Dig J Nanomater Biostruct 2016;11:81-9.
  • Sharma A, Karn RK, Pandiyan SK. Synthesis of TiO2 nanoparticles by sol-gel method and their characterization. J Basic and Appl Eng Res 2014;1:1-5.
  • Toyoda M, Nanbu Y, Nakazawa Y, Hirano M, Inagaki M. Effect of crystallinity of anatase on photoactivity for methyleneblue decomposition in water. Appl Catal B 2004;49: 227-32.
  • Kaygili O, Tatar C, Keser S, Bulut N. Preparation and characterization of monetites co-doped with Ni/Al, Ni/Mn and Al/Mn. Mater Lett 2017;201:39-42.
  • Cullity BD. Elements of X–ray diffraction. Massachusetts: Addison–Wesley Publishing Company;1978.
  • Mote VD, Purushotham Y, Dole BN. Williamson-Hall analysis in estimation of lattice strain in nanometer-sized ZnO particles. J Theor Appl Phys 2012;6:1-8.
  • Bakri AS, Sahdan MZ, Adriyanto F, Raship NA, Said NDM, Abdullah SA, Rahim MS. Effect of annealing temperature of titanium dioxide thin films on structural and electrical properties. International Conference on Engineering, Science and Nanotechnology 2016 (ICESNANO 2016), AIP Conference Proceedings 2017;1788:030030.
  • Hanaor DAH, Sorrell CC. Review of the anatase to rutile phase transformation. J Mater Sci 2011;46:855-74.

Year 2017, Volume: 1 Issue: 2, 38 - 40, 12.12.2017

Omer Kaygili Niyazi Bulut Cengiz Tatar Tankut Ates Turan İnce

Abstract

References

  • Chimupala Y, Hyett G, Simpson R, Mitchell R, Douthwaite R, Milne SJ, Brydson RD. Synthesis and characterization of mixed phase anatase TiO2 and sodium-doped TiO2(B) thin films by low pressure chemical vapour deposition (LPCVD). RSC Adv 2014;4:48507-15.
  • Viana MM, Soares VF, Mohallem NDS. Synthesis and characterization of TiO2 nanoparticles. Ceram Int 2010;36:2047-53.
  • Dadkhah M, Salavati-Niasari M, Mir N. Synthesis and characterization of TiO2 nanoparticles by using new shape controllers and its application in dye sensitized solar cells. J Ind Eng Chem 2014;20:4039-44.
  • Paunović P, Grozdanov A, Češnovar A, Makreski P, Gentile G, Ranguelov B, Fidančevska E. Characterization of nanoscaled TiO2 produced by simplified sol–gel method using organometallic precursor. J Eng Mater Technol 2015;137:021003 1-5.
  • Byranvand MM, Kharat AN, Fatholahi L, Beiranvand ZM. A review on synthesis of nano-TiO2 via different methods. J Nanostruct 2013;3:1-9.
  • Li Z, Kawashita M, Doi M. Sol–gel synthesis and characterization of magnetic TiO2 microspheres. J Ceram Soc Jpn 2010;118:467-73.
  • Chen X, Mao SS. Titanium dioxide nanomaterials: Synthesis, properties, modifications, and applications. Chem Rev 2007;107:2891-959.
  • Phonkhokkong T, Thongtem T, Thongtem S, Phuruangrat A, Promnopas W. Synthesis and characterization of TiO2 nanopowders for fabrication of dye sensitized solar cells. Dig J Nanomater Biostruct 2016;11:81-9.
  • Sharma A, Karn RK, Pandiyan SK. Synthesis of TiO2 nanoparticles by sol-gel method and their characterization. J Basic and Appl Eng Res 2014;1:1-5.
  • Toyoda M, Nanbu Y, Nakazawa Y, Hirano M, Inagaki M. Effect of crystallinity of anatase on photoactivity for methyleneblue decomposition in water. Appl Catal B 2004;49: 227-32.
  • Kaygili O, Tatar C, Keser S, Bulut N. Preparation and characterization of monetites co-doped with Ni/Al, Ni/Mn and Al/Mn. Mater Lett 2017;201:39-42.
  • Cullity BD. Elements of X–ray diffraction. Massachusetts: Addison–Wesley Publishing Company;1978.
  • Mote VD, Purushotham Y, Dole BN. Williamson-Hall analysis in estimation of lattice strain in nanometer-sized ZnO particles. J Theor Appl Phys 2012;6:1-8.
  • Bakri AS, Sahdan MZ, Adriyanto F, Raship NA, Said NDM, Abdullah SA, Rahim MS. Effect of annealing temperature of titanium dioxide thin films on structural and electrical properties. International Conference on Engineering, Science and Nanotechnology 2016 (ICESNANO 2016), AIP Conference Proceedings 2017;1788:030030.
  • Hanaor DAH, Sorrell CC. Review of the anatase to rutile phase transformation. J Mater Sci 2011;46:855-74.
There are 15 citations in total.

Details

Subjects Engineering
Journal Section Articles
Authors

Omer Kaygili

Niyazi Bulut

Cengiz Tatar This is me

Tankut Ates

Turan İnce

Publication Date December 12, 2017
Submission Date December 12, 2017
Published in Issue Year 2017 Volume: 1 Issue: 2

Cite

APA Kaygili, O., Bulut, N., Tatar, C., Ates, T., et al. (2017). Sol-gel synthesis and characterization of TiO2 powder. International Journal of Innovative Engineering Applications, 1(2), 38-40.
AMA Kaygili O, Bulut N, Tatar C, Ates T, İnce T. Sol-gel synthesis and characterization of TiO2 powder. IJIEA. December 2017;1(2):38-40.
Chicago Kaygili, Omer, Niyazi Bulut, Cengiz Tatar, Tankut Ates, and Turan İnce. “Sol-Gel Synthesis and Characterization of TiO2 Powder”. International Journal of Innovative Engineering Applications 1, no. 2 (December 2017): 38-40.
EndNote Kaygili O, Bulut N, Tatar C, Ates T, İnce T (December 1, 2017) Sol-gel synthesis and characterization of TiO2 powder. International Journal of Innovative Engineering Applications 1 2 38–40.
IEEE O. Kaygili, N. Bulut, C. Tatar, T. Ates, and T. İnce, “Sol-gel synthesis and characterization of TiO2 powder”, IJIEA, vol. 1, no. 2, pp. 38–40, 2017.
ISNAD Kaygili, Omer et al. “Sol-Gel Synthesis and Characterization of TiO2 Powder”. International Journal of Innovative Engineering Applications 1/2 (December 2017), 38-40.
JAMA Kaygili O, Bulut N, Tatar C, Ates T, İnce T. Sol-gel synthesis and characterization of TiO2 powder. IJIEA. 2017;1:38–40.
MLA Kaygili, Omer et al. “Sol-Gel Synthesis and Characterization of TiO2 Powder”. International Journal of Innovative Engineering Applications, vol. 1, no. 2, 2017, pp. 38-40.
Vancouver Kaygili O, Bulut N, Tatar C, Ates T, İnce T. Sol-gel synthesis and characterization of TiO2 powder. IJIEA. 2017;1(2):38-40.
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