Research Article
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Spark Plasma Sintering of Nano Silicon Carbide Reinforced Alumina Ceramic Composites

Year 2021, Volume: 5 Issue: 2, 64 - 70, 20.06.2021
https://doi.org/10.26701/ems.841961

Abstract

Although Al2O3 has been commercially preferred material, it cannot be used in applications subject to variable and sudden loads due to its low fracture toughness. In this study, as the primary purpose, to improve the fracture toughness of the Al2O3/nano-SiC particles was used as reinforcement phase. Ultrasonic dispersion was used to ensure good dispersion of the nano reinforcement phase in the matrix. Production was carried out by spark plasma sintering method at temperatures of 1325 °C for 5 min under 40 MPa pressure and vacuum atmosphere. After production process, sintering behavior, density, microstructure, phase structure, hardness and fracture toughness of the Al2O3/nano-SiC composites were analyzed. The highest hardness and fracture toughness of 22.83 GPa and 6.09 MPa·m1/2 was achieved, respectively.

Supporting Institution

Hakkari University Scientific Research Projects Unit

Project Number

FM2017BAP10

Thanks

This work was supported by the Hakkari University Scientific Research Projects Unit (project number: FM2017BAP10). The author thank to Prof. Dr. Gultekin Goller for his contributions.

References

  • Pravarthana, D., Chateigner, D., Lutterotti, L., Lacotte, M., Marinel, S., Dubos, P.A., et al., (2013). Growth and texture of spark plasma sintered Al2O3 ceramics: A combined analysis of X-rays and electron back scatter diffraction. Journal of Applied Physics. 113(15): 153510. doi: 10.1063/1.4802439.
  • Saheb, N., Hayat, U., Hassan, S.F., (2019). Recent advances and future prospects in spark plasma sintered alumina hybrid nanocomposites. Nanomaterials. 9(11): 1–43. doi: 10.3390/nano9111607.
  • Liu, J., Li, Z., Yan, H., Jiang, K., (2014). Spark plasma sintering of alumina composites with graphene platelets and silicon carbide nanoparticles. Advanced Engineering Materials. 16(9): 1111–8. doi: 10.1002/adem.201300536.
  • Liu, J., Yan, H., Jiang, K., (2013). Mechanical properties of graphene platelet-reinforced alumina ceramic composites. Ceramics International. 39(6): 6215–21. doi: 10.1016/j.ceramint.2013.01.041.
  • Ahmad, K., Pan, W., (2015). Microstructure-toughening relation in alumina based multiwall carbon nanotube ceramic composites. Journal of the European Ceramic Society. 35(2): 663–71. doi: 10.1016/j.jeurceramsoc.2014.08.044.
  • Akin, I., (2015). Investigation of the microstructure, mechanical properties and cell viability of zirconia-toughened alumina composites reinforced with carbon nanotubes. Journal of the Ceramic Society of Japan. 123(1437): 405–13. doi: 10.2109/jcersj2.123.405.
  • Chakravarty, D., Bysakh, S., Muraleedharan, K., Rao, T.N., Sundaresan, R., (2008). Spark plasma sintering of magnesia-doped alumina with high hardness and fracture toughness. Journal of the American Ceramic Society. 91(1): 203–8. doi: 10.1111/j.1551-2916.2007.02094.x.
  • Ormanci, O., Akin, I., Sahin, F., Yucel, O., Simon, V., Cavalu, S., et al., (2014). Spark plasma sintered Al2O3-YSZ-TiO2 composites: Processing, characterization and in vivo evaluation. Materials Science and Engineering C. 40: 16–23. doi: 10.1016/j.msec.2014.03.041.
  • Rattanachan, S., Miyashita, Y., Mutoh, Y., (2003). Microstructure and fracture toughness of a spark plasma sintered Al2O3-based composite with BaTiO3 particulates. Journal of the European Ceramic Society. 23(8): 1269–76. doi: 10.1016/S0955-2219(02)00294-7.
  • Razavi, M., Farajipour, A.R., Zakeri, M., Rahimipour, M.R., Firouzbakht, A.R., (2017). Production of Al2O3-SiC nano-composites by spark plasma sintering. Boletin de La Sociedad Espanola de Ceramica y Vidrio. 56(4): 186–94. doi: 10.1016/j.bsecv.2017.01.002.
  • Álvarez, I., Torrecillas, R., Solis, W., Peretyagin, P., Fernández, A., (2016). Microstructural design of Al2O3–SiC nanocomposites by Spark Plasma Sintering. Ceramics International. 42(15): 17248–53. doi: 10.1016/j.ceramint.2016.08.019.
  • Alweendo, S.T., Johnson, O.T., Shongwe, B.M., Kavishe, F.P., Borode, J.O., (2020). Microstructural and mechanical properties of alumina (Al2O3) matrix composites reinforced with SiC from rice husk by spark plasma sintering. Materials Research. 23(1): 1–9. doi: 10.1590/1980-5373-MR-2019-0363.
  • Anstis, G.R., Chantikul, P., Lawn, B.R., Marshall, D.B., (1981). A Critical Evaluation of Indentation Techniques for Measuring Fracture Toughness: I, Direct Crack Measurements. Journal of the American Ceramic Society. 64(9): 533–8. doi: https://doi.org/10.1111/j.1151-2916.1981.tb10320.x.
  • Shi, X.L., Xu, F.M., Zhang, Z.J., Dong, Y.L., Tan, Y., Wang, L., et al., (2010). Mechanical properties of hot-pressed Al2O3/SiC composites. Materials Science and Engineering A. 527(18–19): 4646–9. doi: 10.1016/j.msea.2010.03.035.
  • Torosyan, K.S., Sedegov, A.S., Kuskov, K. V., Abedi, M., Arkhipov, D.I., Kiryukhantsev-Korneev, P. V., et al., (2020). Reactive, nonreactive, and flash spark plasma sintering of Al2O3/SiC composites—A comparative study. Journal of the American Ceramic Society. 103(1): 520–30. doi: 10.1111/jace.16734.
  • Whitney, D.L., Broz, M., Cook, R.F., (2007). Hardness, toughness, and modulus of some common metamorphic minerals. American Mineralogist. 92(2–3): 281–8. doi: 10.2138/am.2007.2212.
Year 2021, Volume: 5 Issue: 2, 64 - 70, 20.06.2021
https://doi.org/10.26701/ems.841961

Abstract

Project Number

FM2017BAP10

References

  • Pravarthana, D., Chateigner, D., Lutterotti, L., Lacotte, M., Marinel, S., Dubos, P.A., et al., (2013). Growth and texture of spark plasma sintered Al2O3 ceramics: A combined analysis of X-rays and electron back scatter diffraction. Journal of Applied Physics. 113(15): 153510. doi: 10.1063/1.4802439.
  • Saheb, N., Hayat, U., Hassan, S.F., (2019). Recent advances and future prospects in spark plasma sintered alumina hybrid nanocomposites. Nanomaterials. 9(11): 1–43. doi: 10.3390/nano9111607.
  • Liu, J., Li, Z., Yan, H., Jiang, K., (2014). Spark plasma sintering of alumina composites with graphene platelets and silicon carbide nanoparticles. Advanced Engineering Materials. 16(9): 1111–8. doi: 10.1002/adem.201300536.
  • Liu, J., Yan, H., Jiang, K., (2013). Mechanical properties of graphene platelet-reinforced alumina ceramic composites. Ceramics International. 39(6): 6215–21. doi: 10.1016/j.ceramint.2013.01.041.
  • Ahmad, K., Pan, W., (2015). Microstructure-toughening relation in alumina based multiwall carbon nanotube ceramic composites. Journal of the European Ceramic Society. 35(2): 663–71. doi: 10.1016/j.jeurceramsoc.2014.08.044.
  • Akin, I., (2015). Investigation of the microstructure, mechanical properties and cell viability of zirconia-toughened alumina composites reinforced with carbon nanotubes. Journal of the Ceramic Society of Japan. 123(1437): 405–13. doi: 10.2109/jcersj2.123.405.
  • Chakravarty, D., Bysakh, S., Muraleedharan, K., Rao, T.N., Sundaresan, R., (2008). Spark plasma sintering of magnesia-doped alumina with high hardness and fracture toughness. Journal of the American Ceramic Society. 91(1): 203–8. doi: 10.1111/j.1551-2916.2007.02094.x.
  • Ormanci, O., Akin, I., Sahin, F., Yucel, O., Simon, V., Cavalu, S., et al., (2014). Spark plasma sintered Al2O3-YSZ-TiO2 composites: Processing, characterization and in vivo evaluation. Materials Science and Engineering C. 40: 16–23. doi: 10.1016/j.msec.2014.03.041.
  • Rattanachan, S., Miyashita, Y., Mutoh, Y., (2003). Microstructure and fracture toughness of a spark plasma sintered Al2O3-based composite with BaTiO3 particulates. Journal of the European Ceramic Society. 23(8): 1269–76. doi: 10.1016/S0955-2219(02)00294-7.
  • Razavi, M., Farajipour, A.R., Zakeri, M., Rahimipour, M.R., Firouzbakht, A.R., (2017). Production of Al2O3-SiC nano-composites by spark plasma sintering. Boletin de La Sociedad Espanola de Ceramica y Vidrio. 56(4): 186–94. doi: 10.1016/j.bsecv.2017.01.002.
  • Álvarez, I., Torrecillas, R., Solis, W., Peretyagin, P., Fernández, A., (2016). Microstructural design of Al2O3–SiC nanocomposites by Spark Plasma Sintering. Ceramics International. 42(15): 17248–53. doi: 10.1016/j.ceramint.2016.08.019.
  • Alweendo, S.T., Johnson, O.T., Shongwe, B.M., Kavishe, F.P., Borode, J.O., (2020). Microstructural and mechanical properties of alumina (Al2O3) matrix composites reinforced with SiC from rice husk by spark plasma sintering. Materials Research. 23(1): 1–9. doi: 10.1590/1980-5373-MR-2019-0363.
  • Anstis, G.R., Chantikul, P., Lawn, B.R., Marshall, D.B., (1981). A Critical Evaluation of Indentation Techniques for Measuring Fracture Toughness: I, Direct Crack Measurements. Journal of the American Ceramic Society. 64(9): 533–8. doi: https://doi.org/10.1111/j.1151-2916.1981.tb10320.x.
  • Shi, X.L., Xu, F.M., Zhang, Z.J., Dong, Y.L., Tan, Y., Wang, L., et al., (2010). Mechanical properties of hot-pressed Al2O3/SiC composites. Materials Science and Engineering A. 527(18–19): 4646–9. doi: 10.1016/j.msea.2010.03.035.
  • Torosyan, K.S., Sedegov, A.S., Kuskov, K. V., Abedi, M., Arkhipov, D.I., Kiryukhantsev-Korneev, P. V., et al., (2020). Reactive, nonreactive, and flash spark plasma sintering of Al2O3/SiC composites—A comparative study. Journal of the American Ceramic Society. 103(1): 520–30. doi: 10.1111/jace.16734.
  • Whitney, D.L., Broz, M., Cook, R.F., (2007). Hardness, toughness, and modulus of some common metamorphic minerals. American Mineralogist. 92(2–3): 281–8. doi: 10.2138/am.2007.2212.
There are 16 citations in total.

Details

Primary Language English
Subjects Mechanical Engineering
Journal Section Research Article
Authors

Mustafa Güven Gök 0000-0002-5959-0549

Project Number FM2017BAP10
Publication Date June 20, 2021
Acceptance Date January 15, 2021
Published in Issue Year 2021 Volume: 5 Issue: 2

Cite

APA Gök, M. G. (2021). Spark Plasma Sintering of Nano Silicon Carbide Reinforced Alumina Ceramic Composites. European Mechanical Science, 5(2), 64-70. https://doi.org/10.26701/ems.841961
AMA Gök MG. Spark Plasma Sintering of Nano Silicon Carbide Reinforced Alumina Ceramic Composites. EMS. June 2021;5(2):64-70. doi:10.26701/ems.841961
Chicago Gök, Mustafa Güven. “Spark Plasma Sintering of Nano Silicon Carbide Reinforced Alumina Ceramic Composites”. European Mechanical Science 5, no. 2 (June 2021): 64-70. https://doi.org/10.26701/ems.841961.
EndNote Gök MG (June 1, 2021) Spark Plasma Sintering of Nano Silicon Carbide Reinforced Alumina Ceramic Composites. European Mechanical Science 5 2 64–70.
IEEE M. G. Gök, “Spark Plasma Sintering of Nano Silicon Carbide Reinforced Alumina Ceramic Composites”, EMS, vol. 5, no. 2, pp. 64–70, 2021, doi: 10.26701/ems.841961.
ISNAD Gök, Mustafa Güven. “Spark Plasma Sintering of Nano Silicon Carbide Reinforced Alumina Ceramic Composites”. European Mechanical Science 5/2 (June 2021), 64-70. https://doi.org/10.26701/ems.841961.
JAMA Gök MG. Spark Plasma Sintering of Nano Silicon Carbide Reinforced Alumina Ceramic Composites. EMS. 2021;5:64–70.
MLA Gök, Mustafa Güven. “Spark Plasma Sintering of Nano Silicon Carbide Reinforced Alumina Ceramic Composites”. European Mechanical Science, vol. 5, no. 2, 2021, pp. 64-70, doi:10.26701/ems.841961.
Vancouver Gök MG. Spark Plasma Sintering of Nano Silicon Carbide Reinforced Alumina Ceramic Composites. EMS. 2021;5(2):64-70.

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